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Ultrafiltration

Ultrafiltration is a membrane stage that retains everything larger than the pores of the membrane: suspended solids, colloids and micro-organisms. Separation is by size, and the retention threshold is from 0.1 down to 0.01 µm. Dissolved matter — hardness salts, nitrates, the salinity as a whole — passes through such a membrane unchanged.

  1. Coarse strainer
  2. Reagent-free filtration
  3. Reagent dosing
  4. Ultrafiltration
  5. Reverse osmosis
  6. Storage tank
  7. UV disinfection

Principle

How it works

The working element of the unit is a hollow-fibre membrane module: a bundle of hollow fibres whose wall is a porous partition. In the units of the catalogue the fibres work inside-out: feed water is delivered into the inner channel of the fibre and leaves through its wall, and the filtrate is collected in the module housing. The governing parameter of the range is not the size of the vessel but the total membrane area: the smaller models carry two modules of some 27 m² in total, the 5 m³/h models four modules of 54.8 m², and the area grows further along with capacity.

The driving force is the pressure difference across the fibre wall, known as the transmembrane pressure. It is modest: the working pressure of the catalogue models lies within 0.2–0.4 MPa, whereas reverse osmosis on fresh water calls for 1.0–1.3 MPa. The reason lies not in the strength of the membrane but in the physics of the process: there is no osmotic pressure to overcome here at all, since dissolved salts pass through the pores and create no difference in concentration across the membrane. Hence the several-fold difference in energy consumption between the two membrane technologies.

What is retained does not leave the apparatus by itself: it builds up on the fibre wall as a layer that raises the transmembrane pressure. The layer is removed by backwashing — filtrate is driven through the wall in the reverse direction and flushes the deposit to drain. A backwash is started by timer or on reaching a set differential, takes tens of seconds and repeats in every cycle. During a backwash the unit delivers no filtrate, and that is covered either by a storage tank or by spare capacity.

Flux through a porous membrane is inversely proportional to the viscosity of the water, and viscosity depends on temperature: at one and the same transmembrane pressure cold water yields less filtrate than warm water. The permissible water temperature for the catalogue models is from 5 to 40 °C, and the size is chosen for the winter minimum rather than for the annual mean: a unit sized on summer water does not reach the required flow in winter.

Fouling divides into reversible and irreversible, and the maintenance regime follows from that. A loose layer of solids is removed by backwashing with water; mineral scale and biofilm are not, and they call for chemical regeneration — a backwash with reagent added, or a full clean with circulating solutions. Acid dissolves the mineral part, alkali and sodium hypochlorite lift organics and biological growth. The pH permitted during cleaning is wider than in service: from 2 to 12, against a working range of 3 to 9.

Principle

The counterintuitive part

A hollow-fibre module works in two fundamentally different hydraulic modes, and the choice of mode changes both the water spent on the unit's own needs and the limiting turbidity of the feed. In dead-end mode all the water supplied leaves as filtrate while what is retained accumulates on the fibre and is removed by periodic backwashing: there is no continuous reject, the share of water spent on own needs is small, but the feed water has to be comparatively clean. In cross-flow mode part of the stream travels along the fibre and carries the retained matter away continuously: a continuous reject appears, water and energy consumption rise, but the apparatus tolerates markedly more turbid and more heavily loaded water. One and the same size delivers a different filtrate capacity in these two modes, so the mode is fixed by calculation before ordering rather than settled during commissioning.

An ultrafiltration membrane is cleaned with sodium hypochlorite — the very reagent that irreversibly destroys the polyamide active layer of a reverse osmosis element at concentrations of the order of 0.1 mg/l. The difference in the chemical resistance of the materials is fundamental here, and two practical conclusions follow from it. Ultrafiltration tolerates water with residual free chlorine and is therefore applicable directly downstream of a chlorinated source. At the same time the pairing of ultrafiltration with reverse osmosis does not remove the need for dechlorination: the resistance of the first membrane does not extend to the second, and an adsorption stage or the dosing of a reducing agent between them remains obligatory.

How clear the water looks says nothing about its suitability for membrane desalination. The danger comes from colloids — particles of a fraction of a micrometre that neither settle nor are visible; their content is assessed by the silt density index SDI, measured on a separate 0.45 µm membrane, and for polyamide elements it is usually kept below 5. A 5 µm cartridge does not lower that index at all — colloids pass straight through it — while granular filtration of surface water gives a result that shifts with floods and algal blooms. Ultrafiltration does lower SDI, because its retention threshold is two orders of magnitude finer, and that is precisely its role as pretreatment: it does not improve the water in general, it makes one specific parameter predictable at the inlet of the membrane unit.

Practice

What that gives in practice

Ultrafiltration closes the undissolved part of the task entirely and in terms of result replaces the pairing of settling and microfiltration — two units that take up floor space and require attention. The quality of the filtrate is set by the retention threshold rather than by a settling regime, so seasonal changes in the source do not show at the outlet: a flood, an algal bloom or stirred-up sediment after works on the mains change the frequency of backwashes, not the turbidity of the treated water.

The second typical role of the stage is pretreatment ahead of reverse osmosis on difficult water. The economics of such a scheme are counted not by the cost of the unit but by the service life of the osmosis elements and by the number of chemical cleans per year: the less stable the source, the sooner ultrafiltration pays for itself. One reservation is essential: it removes the load of suspended solids and colloids only, while hardness salts, silica and alkalinity reach the osmosis stage unchanged, so softening or antiscalant dosing does not disappear from the scheme.

The microbiological barrier here is mechanical and calls for neither reagent nor contact time. It is not, however, disinfection in the regulatory sense: the barrier exists exactly as long as the fibres are intact, and a single broken fibre barely shows in flow or pressure and is detected only by monitoring the turbidity of the filtrate. The line downstream of ultrafiltration is therefore closed by ultraviolet disinfection rather than treated as complete.

The requirements on the feed water look different from those of reverse osmosis, but they exist. A coarse strainer ahead of the module is obligatory: sand and large solids damage the fibre mechanically. Iron and manganese must either be within limits or fully oxidised at a preceding stage — in dissolved form they pass through the membrane, and as they oxidise inside the pores and on the fibre wall they leave deposits that backwashing no longer removes.

The unit is supplied assembled on a frame and comprises the membrane modules, a pump, a prefilter, the backwash assembly, instrumentation and a mode controller. The site has to provide a heated room at 5 to 35 °C, a feed water connection of the design flow, a drain line for backwash water, power supply and access for servicing the modules. We do not manufacture this equipment: our part of the work is the water analysis, the calculation of the scheme and of the membrane area, the choice of size and mode, supply, commissioning and subsequent service.

Limits

When you need it

  • The source is a surface one — a river, a reservoir, a lake: turbidity and colour change with the season while the salinity stays within limits.
  • Consistent clarified water quality is required regardless of floods, algal blooms and works on the mains, rather than an acceptable annual average.
  • A microbiological barrier independent of reagent dose is needed: a hotel, a food production line, a municipal or group water supply.
  • Reverse osmosis is planned on water with an unstable silt density index SDI, and the desalination elements have to be protected from suspended solids and colloids.
  • The task is the polishing of biologically treated effluent or a water recycling loop: retention of suspended solids, fats and insoluble oil products before the water returns to the cycle.
  • Floor space for water treatment is limited, and a settling unit followed by microfiltration either does not fit the room or demands an unacceptable amount of attention.

When it will not help

  • Where the exceedances in the analysis relate to salinity, hardness, nitrates or fluorides. Ultrafiltration does not reduce these parameters at all: the substances listed are dissolved, and separation here is by size. The task is solved by reverse osmosis.
  • Where water of a constant mineral composition is required for a beverage recipe or a food line. Ultrafiltration makes the water clear, but its mineral composition stays equal to that of the feed and shifts along with the source.
  • Where deep borehole water is clear and the exceedances relate to iron, manganese or hydrogen sulphide. Reagent-free filtration with aeration solves such a task far more cheaply; without prior oxidation ultrafiltration does not retain iron, it merely receives it onto the fibre as a deposit.
  • Where disinfection is required as a regulated result in its own right. The membrane is a barrier by size but provides no regulated dose; ultraviolet disinfection or chlorination is installed downstream of it.
  • Where the site cannot provide the conditions for operation: a heated room, a drain line for backwash water, access to the modules for servicing. Freezing of a module is irreversible, as is drying out of the membrane during a long shutdown without preservation.

Practice

Typical cases

Feed
A surface intake: turbidity from 3 to 40 mg/l over the season, elevated colour, salinity around 250 mg/l, water temperature from 6 °C in winter to 22 °C in summer.
Task
To supply 20 m³/h of clarified water of consistent quality to a hotel complex, hot water service included.
Scheme
Coarse strainer → ultrafiltration in dead-end mode with backwashing on differential pressure → storage tank → ultraviolet disinfection.
Result
The turbidity of the filtrate stays low in any seasonal state of the source. Salinity and hardness remain as they were in the feed — the task did not call for changing them. The size was chosen for the winter temperature and for the seasonal turbidity peak, on which the frequency of backwashes depends.
Feed
River water ahead of a desalination unit: during floods the silt density index SDI exceeds 6 and shifts within the day, salinity 1200 mg/l, hardness 6 meq/l.
Task
To obtain 10 m³/h of desalinated water while keeping the interval between chemical cleans of the osmosis elements within acceptable limits.
Scheme
Coarse strainer → ultrafiltration → antiscalant dosing → reverse osmosis of the brackish water series → storage tank → ultraviolet disinfection.
Result
The silt density index at the inlet of the membrane unit becomes predictable and stops depending on the season, and the number of chemical cleans of the osmosis stage falls. The antiscalant stays in the scheme: ultrafiltration does not retain hardness salts and removes no risk of carbonate scaling in the concentrate line.
Feed
Biologically treated effluent downstream of the secondary clarifier: suspended solids from 10 to 25 mg/l, residual organics, a requirement to return the water to the process cycle.
Task
To prepare water for a recycling loop serving washing operations, where the original salinity is acceptable but suspended solids and biological growth are not.
Scheme
Equalisation → coarse strainer → ultrafiltration in cross-flow mode → storage tank → ultraviolet disinfection.
Result
Suspended solids and insoluble oil products are retained and the water returns to the cycle. Cross-flow mode was chosen because of the solids load: it produces a continuous reject and a higher share of water spent on own needs, but it allows work on water on which dead-end mode would go into continuous backwashing.

The cases are typical examples, not site reports.

Innovations

Our developments for this stage

Scheme

Place in the scheme

Unlike reverse osmosis, ultrafiltration can be a stage in its own right: where the task is confined to turbidity, colour of suspended origin and microbiology, the scheme consists of a strainer, the unit, a storage tank and disinfection. A coarse strainer is obligatory in every case: it protects the fibre from sand and large solids.

The requirements on the feed water are stated in figures rather than in words: limiting turbidity and suspended solids to suit the chosen mode of operation, temperature from 5 to 40 °C, pH from 3 to 9, iron and manganese either within limits or fully oxidised at a preceding stage. Free chlorine, unlike in schemes built around polyamide membranes, is permissible here.

In combination with desalination the order of the stages admits no rearrangement: ultrafiltration comes first and removes suspended solids and colloids, while dechlorination and antiscalant dosing or softening remain between it and the osmosis stage. The reverse order makes no sense: the osmosis stage would receive the whole colloidal load for the removal of which the stage is installed.

The backwash water line is treated as part of the scheme rather than as an auxiliary drain. It is sized on the instantaneous backwash flow rather than on the average share, because the discharge comes in bursts. Cleans with reagent call for neutralisation of the solution discharged; the discharge point and its limits are agreed with the water and sewerage authority before the equipment is ordered.

Scheme

Automation and control

  • Monitoring of the transmembrane pressure. Its rise at unchanged flow is the grounds for a backwash and the principal indicator of the state of the modules; the residual differential after a chemical clean shows the share of irreversible fouling.
  • Monitoring of filtrate turbidity. It is the only sign that the integrity of a fibre has been lost: a single broken fibre barely shows in flow or pressure, whereas the quality of the filtrate is lost at once.
  • Cycle control: filtration, forward flush and backwash are switched by the controller on a timer or on reaching a set differential. Cleans with reagent added are run to a schedule tied to the actual load rather than to the calendar.
  • A cut-out on limiting pressure. Exceeding the design value damages the fibre irreversibly, so the shutdown is automatic and does not depend on the operator.
  • Shutdown on the level in the storage tank, on low inlet pressure and on drive overload, together with a preservation regime for a long stoppage: the membrane must not dry out, and where the room can fall below freezing the modules are to be drained.

Operation

Running it

Energy

The specific power consumption is set by the working pressure and is therefore modest: at 0.2–0.4 MPa and with backwashes taken into account it comes to some 0.1–0.2 kWh per cubic metre of filtrate. The exact figure depends on pump efficiency, on losses in the pipework and on the frequency of backwashes, which rises with the turbidity of the feed. For comparison, reverse osmosis on fresh water consumes 0.3–0.8 kWh per cubic metre of permeate, and the difference is explained not by the design but by the fact that no osmotic pressure has to be overcome here.

Consumables

  • Cartridges or the screen of the prefilter: the servicing interval is set by differential pressure, not by a calendar date
  • Cleaning chemicals — acid, alkali, sodium hypochlorite: consumption follows the number of cleans, and that depends on the load of solids and organics
  • Reagents for neutralising the spent cleaning solution, where the discharge has to be brought to an agreed pH
  • Membrane modules: replaced on actual condition — on a rise in transmembrane pressure that a chemical clean no longer restores, rather than by the calendar

What goes to drain

Backwash water contains everything retained in a reduced volume: suspended solids, colloids, biomass and the organics bound up with them. The discharge comes in bursts, so the line is sized on the instantaneous backwash flow rather than on the averaged share: that instantaneous flow is of the order of 10–20 % of the feed. After cleans with reagent the discharge additionally calls for neutralisation — the working solutions of chemical regeneration have a pH of between 2 and 12. The discharge point and its limits are agreed in advance, and they differ from site to site.

Recovery

What ultrafiltration spends on its own needs is backwash water. In dead-end mode a backwash is short and periodic, so the share averaged over the cycle usually comes to a few per cent, even though the instantaneous flow of the backwash itself reaches 10–20 % of the feed. The figure is not a constant: it rises with the turbidity of the feed water, since dirty water calls for more frequent backwashes, and it is markedly higher in cross-flow mode, where a continuous reject is added to the backwashes. The flow should be counted at the inlet rather than at the filtrate, and that requirement falls on the source rather than on the unit.

Sizing

Sizing

What we account for

  • An analysis of the feed water with its seasonal limits: turbidity and its flood peak, suspended solids, colour, permanganate oxidisability, iron and manganese, microbiology, winter temperature
  • The silt density index SDI, where the stage is installed as pretreatment ahead of desalination: it is what sets the required retention threshold and the margin in membrane area
  • The required filtrate flow and the mode of operation: hours per day, peak draw-offs and whether the breaks for backwashing, during which the unit delivers nothing, are acceptable
  • The mode of the modules — dead-end or cross-flow: it is chosen by the load of the feed water and directly changes the capacity of one and the same size
  • Inlet pressure and temperature, the presence of a booster pump and the seasonal limits within which they vary
  • The conditions for discharging backwash water: instantaneous flow, the bursty nature of the discharge, the possibility of neutralising chemical regeneration solutions
  • The characteristics of the site: room for the frame and the storage tank, ceiling height, heating, power supply, access for servicing and replacing the modules

What a wrong choice costs

  • Sizing on the annual mean turbidity. A unit sized on average water goes into frequent backwashing during a flood: the share of water spent on own needs rises and the actual filtrate capacity falls exactly when the water is needed most.
  • Counting the requirement at the feed instead of at the filtrate. During a backwash the unit delivers no water, and without a storage tank or spare capacity the consumer sees dips in flow that the data sheet figure does not show.
  • Ultrafiltration instead of desalination. The result is clear water of the same hardness and the same salinity: the task the equipment was ordered for is not solved at all, and a second membrane stage is required.
  • Unoxidised iron ahead of the membrane. In dissolved form it passes through the module, but it oxidises inside the pores and on the fibre wall, and such deposits are no longer removed by backwashing and cut the service life of the modules to a few months.
  • The absence of a coarse strainer. Sand and large solids damage the fibre mechanically, and the damage is irreversible: the integrity of a module cannot be restored by washing.

Sizing

What we need for a calculation

  • A water analysis report: turbidity with its seasonal peak, suspended solids, colour, permanganate oxidisability, iron, manganese, salinity, hardness, microbiology, temperature
  • The type of source and its behaviour through the season: river, reservoir, borehole, mains, treated effluent
  • The required filtrate flow and the mode of operation: hours per day, peak draw-offs, acceptable interruptions
  • The purpose of the water and the stages that follow, where desalination or disinfection is intended downstream of ultrafiltration
  • Inlet water pressure and temperature, and whether a booster pump is present
  • The conditions for discharging backwash water: the instantaneous flow available, the discharge point, limits on pH and composition
  • The characteristics of the site: floor area and ceiling height, heating, power supply, delivery routes, room for the storage tank

Questions

Questions

Ultrafiltration or reverse osmosis?

These are different tasks, not different levels of quality. Ultrafiltration is a porous barrier with a retention threshold from 0.1 to 0.01 µm: it retains suspended solids, colloids and micro-organisms, that is, everything larger than the pores. A reverse osmosis membrane has no through pores at all, transport goes through a dense polymer and separation takes place at the level of ions, which is why salinity falls. The order of decision is simple: take the analysis report and look at two groups of parameters separately. Turbidity, colour, suspended solids and microbiology are the domain of ultrafiltration. Salinity, hardness, nitrates and fluorides are the domain of osmosis. If there are exceedances in both groups the scheme will have two stages, and ultrafiltration will be the first of them.

Will ultrafiltration reduce hardness and salinity?

No, and this is not a question of the degree of treatment. Calcium, magnesium, sodium, nitrates and chlorides are in the dissolved state, whereas separation at this stage is by size, so dissolved matter passes the membrane unchanged. After ultrafiltration brackish water becomes clear and stays brackish, and scale forms in the same amount as before. For these parameters ion exchange or reverse osmosis is used.

Does the membrane replace disinfection?

It does not, although it does create a barrier by size against bacteria. Viruses are retained the more completely the lower the retention threshold of the module, and at 0.1 µm retention is incomplete. Beyond that, the barrier exists exactly as long as the fibres are intact: a single broken fibre barely shows in flow or pressure and is detected only by monitoring filtrate turbidity. The line downstream of the unit is therefore closed by ultraviolet disinfection, and the membrane is regarded as a stage that reduces the load on it rather than one that removes the need for it.

What has to stand ahead of ultrafiltration?

A coarse strainer at the very least: sand and large solids damage the fibre mechanically and irreversibly. What else is needed follows from the analysis. Where the water carries dissolved iron and manganese, their oxidation is completed before the membrane — otherwise they pass through it in ionic form and settle on the fibre from the other side. Free chlorine, unlike in schemes with polyamide reverse osmosis elements, is permissible: ultrafiltration membranes are themselves cleaned with sodium hypochlorite.

How much water goes on the unit's own needs?

In dead-end mode it is backwash water. The instantaneous flow of a backwash is of the order of 10–20 % of the feed, but the backwash itself takes tens of seconds and repeats periodically, so the share averaged over the cycle usually comes to a few per cent. It rises with the turbidity of the feed water, and in cross-flow mode a continuous reject is added to the backwashes, which makes the share markedly higher. The drain line, meanwhile, is sized on the instantaneous flow, since the discharge comes in bursts.

Can ultrafiltration be installed instead of a clarifying filter with granular media?

In terms of result, yes, and on surface water that is often the preferable decision: the quality of the filtrate is set by the retention threshold of the membrane and therefore does not depend on the seasonal state of the source, whereas granular media give a variable result during a flood. The two decisions differ in operation: a membrane stage calls for a controller, a regime of chemical cleans and a drain line, but it takes up less floor space and lowers the silt density index SDI, which a granular filter does not do. The choice is made on the analysis and on the requirements of the stages that follow.

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